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How to choose a suitable crystallizer

2023-04-12
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Consider the characteristics of the solution. Different solutions have different characteristics, such as solubility, crystallization rate, and crystallization temperature. Choosing a suitable crystallizer based on the characteristics of the solution is crucial. Generally speaking, when the solubility is low and the crystallization rate is slow, a larger crystallizer can be selected to obtain more crystals. When the solubility is high and the crystallization rate is fast, a smaller crystallizer can be selected to control the crystallization process.

Consider the material of the crystallizer. The material of the crystallizer will have a certain impact on temperature changes, solute migration, and crystal purity during the crystallization process. Generally speaking, glass crystallizers are commonly used as they have good chemical and thermal stability. However, in some special circumstances, such as the need for high-temperature crystallization or high corrosiveness to specific chemicals, ceramic or metal crystallizers can be chosen.

Consider the shape and size of the crystallizer. The shape and size of the crystallizer directly affect the shape and size of the crystal. Generally speaking, the shape of the crystallizer should match the shape of the desired crystal. For example, if it is necessary to obtain large crystalline particles, a crystallizer with a larger diameter should be selected; If it is necessary to obtain small crystalline particles, a crystallizer with a smaller diameter should be selected. In addition, the height of the crystallizer should also be determined based on the volume of the solution and the yield of crystals.

Consider the special functions of the crystallizer. Some crystallizers have special functions that can improve crystallization efficiency and purity of crystals. For example, a circulating crystallizer can improve crystallization efficiency by continuously circulating the solution; Fixed bed crystallizers can use multiple crystallizers to achieve continuous crystallization processes; Vacuum crystallizers can reduce impurities and harmful gases during the crystallization process. According to the specific requirements of the experiment, choosing a crystallizer with special functions may be more advantageous.

Select a suitable crystallizer based on the laboratory equipment and experimental conditions. The selection of crystallizers should also consider laboratory equipment and experimental conditions. For example, if the laboratory has temperature control equipment, you can choose the crystallizer that needs temperature control; If the laboratory can provide appropriate mixing equipment, the crystallizer that needs to be stirred can be selected. In addition, the budget and time importance of the laboratory should also be considered, and a crystallizer suitable for the laboratory should be selected.


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